Extraction And Characterization Of Oil From Date Seed

Project and Seminar Material for Chemical Engineering

Extraction And Characterization Of Oil From Date Seed


Abstract


The aim of this project is centered on the extraction and characterization of oil from date seed. The extraction is carried out with the use of a soxhlet apparatus and a solvent hexane which is chosen base on the fact that it has a very low value of toxicity and high extraction rate. The different particle size gotten from the gotten from the grinded date seed were 710 um, 1mm and 2mm mesh size, which 40g of each were measured and subjected to the process and they yield the following value of oil respectively 363, 3.49 and 3.25 with the smallest particle size producing the highest yield.


Table of Content


  • Title page
  • Certification
  • Dedication
  • Acknowledgement
  • Abstract
  • Table of Contents

Chapter One:

Introduction

  • 1.1 Background of the Study
  • 1.2 Aim and Object of the Project
  • 1.3 Relevance of Work
  • 1.4 Scope of the Work

Chapter Two:

2.0 Literature Review

  • 2.1 History and Background of Date Seed
  • 2.2 Propagation and Culture
  • 2.4 Fats and Oil
  • 2.5 Location of Oil
  • 2.6 General Properties and Composition of Fat and Oil
  • 2.7 Industrialization of Oil and Fat
  • 2.8 Classification of Nutrient Content
  • 2.9 Date Pollination

Chapter Three:

Raw Materials and Methodology

  • 3.0 Instrumentation and Procedure
  • 3.2 Equipment
  • 3.3 Properties and Value of Hexane
  • 3.4 Toxicity of Hexane
  • 3.5 Extraction by Solvent
  • 3.6 Procedure

Chapter Four:

Result and Discussion

  • 4.0 Result
  • 4.2 Presentation of Result

Chapter Five:

Conclusion and Recommendations

  • 5.1 Conclusion
  • 5.2 Recommendation
  • References

Chapter One


Introduction

1.1 Background of the Study

Oil could be defined as any greasily substance that is liquid at room temperature and is insoluble in water. Oil is derived mainly from two two main sources namely plant and animal. In animal they occur mainly inform of eclipse tissure and all composed of cell, while in plant they are mostly found in storage organs like seed (Abraham et al. 1970). Oil is generally liquid under room or ordinary temperature and those that exist as solid are called fats.

Vegetable oil and fat have a wide range of uses as food for industrial purpose and also in pharmaceuticals.

Dates are low cost source of food with high nutritional value. The date palm is an important member of the family palmacen, providing a staple food for millions of people in arid and semiarid regions of the world. Dates may be considered as almost ideal food, providing a wide range of essential nutrients and potential health benefits. The sugar content of ripe dates is aboiut 80%; the remainder consists of protein, fibre and trace element including born, cobalt, fluorine, magasium, managanese, selenium and zinc.

Extraction may be used to separate more than two components and mixture of solvents. It is also a method of removing one constituent from a solid or liquid by means of liquid solvent. These techniques falls into two categories, the first is called leaching or solid extraction, it is used to dissolve soluble matter from its mixture with an insoluble solid. The second is called liquid extraction is used to recover a valuable product from s multi-component solution by contact with an immiscible solvent that has a high affinity for the product. (W.L. Mcable, J.C. Smith, P.HarrioH, unit operation of chemical engineering seventh (7th) Edition 2005.

Leaching is a process of extracting a substance from a solid by means of dissolving it in a liquid. In the chemical processing industries, leaching is known as extraction. Leaching has a variety of commercial applications which includes the separation of a metal from it ore using acid, separation of sugar from beats using hot water, leaching of chloride from food substances. (Wikipedia, 2006)

In leaching, there are four important factors to be considered which the particles size, solvent temperature and agitation of the fluid. Generally, the process can be considered in three solute as it dissolve in the solvent, its diffusion through the solvent in the pores of the solid to outside of the particles. And the transfer of the solute from the solution in contact with the particles to he main bulk of the solution. And of these process may be responsible for limiting the rapidly that it has a negligible effect on the overall rate (Coulson and Richardson 1990).


1.2 Aim and Objective

The aim of the project is centered on acquiring the general knowledge of separating a particular component from it mixture with other component successfully, while the objective is to carry out the extraction of oil from date seed using the separation method known as leaching.


1.3 Relevance of the Work

The knowledge of extraction of oil from date seed does not only help the students of chemical engineering on how to carryout separation but also the method suitable for anykind of mixture either liquid-solid mixture or liquid-liquid mixture.


1.4 Scope of Study

  1. Extraction of the oil
  2. Determination of the following physiochemical properties of the oil
  3. Iodine value
  4. Saponification value
  5. Acid value
  6. Viscosity
  7. pH value
  8. Unsaponification matter
  9. Specific gravity
  10. Peroxide value
  11. Free fatty acid

Chapter Five


5.0 Conclusion and Recommendation

5.1 Conclusion

The reference sample used for the extraction (leaching) process is grinded date seed that is classified into three particle size ranging from 710min, 1mm and 2mm. The result obtained shown or confirms that the size of the particle is a very important factor that can either increase or decrease the rate of extraction.

The solvent used for the extraction process is hexane which it evaporating or escaping tendency is in between that of petroleum ether and ethanol that is it should not be too high and also not too low. Hexane is less toxic and has a high extraction rate.

Date seed oil may be regarded as oleic-lauric oil because of their high composition in the fatty acid and the low acid content of the oil show that the oil is edible and consumable. However, the low oil content of date seeds (7 to 10%) result in little commercial interest by the oil extraction industry. Date seed oil would appear to be useful in cosmetics pharmaceuticals, soaps and detergent, chemical intermediates and food application.


5.2 Recommendation

At the end of this project experiment the following recommendation are been suggested.

  1. That student should practicalize on the oil by using it in the production of soap and detergent, and cosmetics.
  2. The equipment in the chemical engineering laboratory should be sufficient and available to student toc arry out their practical in due time.

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